The Amazing Spiderman #142 By Marvel Comics.  March 1975. Titled “Dead Man’s Bluff!” Written by Gerry Conway with art by Ross Andru, Frank Giacoia, and Dave Hunt.  32 pages.

Spider-Man dives into the Hudson River to find the Spider-Buggy and wonders over hallucinating or if Mysterio is haunting him.  Mysterio reappears but dissolves once Spider-Man attempts capturing him.

Mysterio Means Madness!  Used.

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